Crystal structure ofcatena-poly[[silver(I)-{μ-2,6-bis[(1H-pyrazol-1-yl)methyl]pyridine-κ3N1,N2:N2′}] nitrate]

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چکیده

منابع مشابه

Crystal structure of catena-poly[[silver(I)-{μ-2,6-bis­[(1H-pyrazol-1-yl)meth­yl]pyridine-κ3 N 1,N 2:N 2′}] nitrate]

In the title complex, {[Ag(C13H13N5)]NO3} n , the Ag(I) atom is coordinated by three N atoms from two bidentate/monodentate pyrazolylpyridyl ligands to form a distorted trigonal-planar geometry [range of angles: 83.34 (6) (chelate ring) to 139.15 (7) °]. The chelate ring has a distorted boat conformation. The dihedral angle between the pyridyl ring and the coordinating pyrazolyl ring is 67.22 (...

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Crystal structure of 1-meth­oxy-2,2,2-tris­(pyrazol-1-yl)ethane

The title compound, C12H14N6O, consists of three pyrazole rings bound via nitro-gen to the distal ethane carbon of meth-oxy ethane. The dihedral angles between the three pyrazole rings are 67.62 (14), 73.74 (14), and 78.92 (12)°. In the crystal, mol-ecules are linked by bifurcated C-H,H⋯N hydrogen bonds, forming double-stranded chains along [001]. The chains are linked via C-H⋯O hydrogen bonds,...

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Crystal structure of di­cyclo­hexyl­ammonium nitrate(V)

In the title mol-ecular salt, C12H24N(+)·NO3 (-), the cyclohexyl rings adopt chair conformations with the exocyclic C-N bonds in equatorial orientations. In the crystal, a bifurcated N-H⋯(O,O) hydrogen bond links the cation to the anion; the ion pairs are linked via C-H⋯O hydrogen bonds, forming layers in the ac plane.

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Crystal structure of 1,4,5,6,7,8,9,10,11,12,13-undeca­hydro­cyclo­dodeca[c]pyrazol-3-ol

The title compound, C13H22N2O, crystallized as a pyrazolol tautomer. The 12-membered macrocycle has a distorted chair conformation. In the crystal, mol-ecules are linked via pairs of O-H⋯N hydrogen bonds, forming inversion dimers. The dimers are linked via N-H⋯π and C-H⋯π inter-actions, forming slabs parallel to the bc plane.

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Crystal structure of 2-[bis(1H-pyrazol-1-yl)meth­yl]pyridine

In the title compound, C13H13N5, the planes of the pyrazolyl groups are nearly perpendicular to that of the central pyridine ring, making dihedral angles of 87.77 (8) and 85.73 (7)°. In the crystal, weak C-H⋯N hydrogen bonds link the mol-ecules into layers extending parallel to (10-1).

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Crystallographic Communications

سال: 2015

ISSN: 2056-9890

DOI: 10.1107/s2056989015004120